Synthesis and Structure of 4-[(anthracene-9′-ylmethylene)amino]-5-R-2,4-Dihydro-3H-1,2,4-Triazole-3-Thiones

By the condensation of 4-amino-5-R-2,4-dihydro-3H-1,2,4-triazole-3-thiones with anthracene-9- carbaldehyde, respective 4-[(anthracene-9′-ylmethylene)amine)]-5-R-2,4-dihydro-3H-1,2,4-triazole-3-thiones are prepared and structurally characterized by NMR, UV, IR spectroscopies, high-resolution mass spe...

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Главные авторы:	Demidov, O. P., Демидов, О. П.
Формат:	Статья
Язык:	English
Опубликовано:	2024
Темы:	4-amino-1,2,4-triazole-3-thione Single crystal X-ray diffraction Anthracene Azomethine ligands
Online-ссылка:	https://dspace.ncfu.ru/handle/123456789/29166
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spelling	ir-123456789-291662024-10-29T14:03:44Z Synthesis and Structure of 4-[(anthracene-9′-ylmethylene)amino]-5-R-2,4-Dihydro-3H-1,2,4-Triazole-3-Thiones Demidov, O. P. Демидов, О. П. 4-amino-1,2,4-triazole-3-thione Single crystal X-ray diffraction Anthracene Azomethine ligands By the condensation of 4-amino-5-R-2,4-dihydro-3H-1,2,4-triazole-3-thiones with anthracene-9- carbaldehyde, respective 4-[(anthracene-9′-ylmethylene)amine)]-5-R-2,4-dihydro-3H-1,2,4-triazole-3-thiones are prepared and structurally characterized by NMR, UV, IR spectroscopies, high-resolution mass spectrometry, and single crystal XRD. The effect of a substituent at position 5 in triazole moieties of azomethines obtained on their head-to-head or head-to-tail crystal packings is determined. 2024-10-29T14:02:58Z 2024-10-29T14:02:58Z 2024 Статья Kolodina A.A., Demidov O.P., Popov L.D., Dubonosova I.V., Khodykina E.S., Skorova A.V., Zaichenko S.B., Borodkina I.G., Dubonosov A.D., Metelitsa A.V., Vlasenko V.G. Synthesis and Structure of 4-[(anthracene-9′-ylmethylene)amino]-5-R-2,4-Dihydro-3H-1,2,4-Triazole-3-Thiones // Journal of Structural Chemistry. - 2024. - 65 (8). - pp. 1631 - 1640. - DOI: 10.1134/S0022476624080146 https://dspace.ncfu.ru/handle/123456789/29166 en Journal of Structural Chemistry application/pdf application/pdf
institution	СКФУ
collection	Репозиторий
language	English
topic	4-amino-1,2,4-triazole-3-thione Single crystal X-ray diffraction Anthracene Azomethine ligands
spellingShingle	4-amino-1,2,4-triazole-3-thione Single crystal X-ray diffraction Anthracene Azomethine ligands Demidov, O. P. Демидов, О. П. Synthesis and Structure of 4-[(anthracene-9′-ylmethylene)amino]-5-R-2,4-Dihydro-3H-1,2,4-Triazole-3-Thiones
description	By the condensation of 4-amino-5-R-2,4-dihydro-3H-1,2,4-triazole-3-thiones with anthracene-9- carbaldehyde, respective 4-[(anthracene-9′-ylmethylene)amine)]-5-R-2,4-dihydro-3H-1,2,4-triazole-3-thiones are prepared and structurally characterized by NMR, UV, IR spectroscopies, high-resolution mass spectrometry, and single crystal XRD. The effect of a substituent at position 5 in triazole moieties of azomethines obtained on their head-to-head or head-to-tail crystal packings is determined.
format	Статья
author	Demidov, O. P. Демидов, О. П.
author_facet	Demidov, O. P. Демидов, О. П.
author_sort	Demidov, O. P.
title	Synthesis and Structure of 4-[(anthracene-9′-ylmethylene)amino]-5-R-2,4-Dihydro-3H-1,2,4-Triazole-3-Thiones
title_short	Synthesis and Structure of 4-[(anthracene-9′-ylmethylene)amino]-5-R-2,4-Dihydro-3H-1,2,4-Triazole-3-Thiones
title_full	Synthesis and Structure of 4-[(anthracene-9′-ylmethylene)amino]-5-R-2,4-Dihydro-3H-1,2,4-Triazole-3-Thiones
title_fullStr	Synthesis and Structure of 4-[(anthracene-9′-ylmethylene)amino]-5-R-2,4-Dihydro-3H-1,2,4-Triazole-3-Thiones
title_full_unstemmed	Synthesis and Structure of 4-[(anthracene-9′-ylmethylene)amino]-5-R-2,4-Dihydro-3H-1,2,4-Triazole-3-Thiones
title_sort	synthesis and structure of 4-[(anthracene-9′-ylmethylene)amino]-5-r-2,4-dihydro-3h-1,2,4-triazole-3-thiones
publishDate	2024
url	https://dspace.ncfu.ru/handle/123456789/29166
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Synthesis and Structure of 4-[(anthracene-9′-ylmethylene)amino]-5-R-2,4-Dihydro-3H-1,2,4-Triazole-3-Thiones

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