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Synthesis of 5-Aryl-4-sulfanylidene-2,3,4,5,6,8-hexahydro-7H-pyrido[3,2-e][1,3]thiazin-7-ones

N-Methylmorpholinium 4-aryl-5-cyano-2-oxo-1,2,3,4-tetrahydropyridine-6-thiolates reacted with hydrogen sulfide and formaldehyde in ethanol to give 5-aryl-4-sulfanylidene-2,3,4,5,6,8-hexahydro-7H-pyrido[3,2-e][1,3]thiazin-7-ones. The molecular and crystal structures of N-methylmorpholinium 5-cyano-2-...

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Wedi'i Gadw mewn:
Manylion Llyfryddiaeth
Prif Awduron: Dotsenko, V. V., Доценко, В. В., Aksenov, N. A., Аксенов, Н. А.
Fformat: Статья
Iaith:English
Cyhoeddwyd: Pleiades Publishing 2024
Pynciau:
Mynediad Ar-lein:https://dspace.ncfu.ru/handle/123456789/29321
Tagiau: Ychwanegu Tag
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Crynodeb:N-Methylmorpholinium 4-aryl-5-cyano-2-oxo-1,2,3,4-tetrahydropyridine-6-thiolates reacted with hydrogen sulfide and formaldehyde in ethanol to give 5-aryl-4-sulfanylidene-2,3,4,5,6,8-hexahydro-7H-pyrido[3,2-e][1,3]thiazin-7-ones. The molecular and crystal structures of N-methylmorpholinium 5-cyano-2-oxo-4-(3,4,5-trimethoxyphenyl)-1,2,3,4-tetrahydropyridine-6-thiolate were determined by X-ray analysis.