Synthesis of yttrium aluminum garnet ceramic powder doped with ruthenium

In the course of the work, samples of ceramic powders of yttrium-aluminum garnet doped with ruthenium ions were obtained. The introduced amount of ruthenium was 5 and 10 wt.%, respectively. The annealing temperatures were 1150 and 1600°C. In the course of the work, changes in the morphology of ceram...

Полное описание

Сохранить в:

Библиографические подробности
Главные авторы:	Suprunchuk, V. E., Супрунчук, В. Е., Kravtsov, A. A., Кравцов, А. А., Tarala, L. V., Тарала, Л. В., Medyanik, E. V., Медяник, Е. В., Malyavin, F. F., Малявин, Ф. Ф., Lapin, V. A., Лапин, В. А., Bedrakov, D. P., Бедраков, Д. П.
Формат:	Статья
Язык:	Russian
Опубликовано:	Tver State University 2025
Темы:	Yttrium aluminum garnet Ruthenium Alloying Ceramic powder Differential thermal analysis
Online-ссылка:	https://dspace.ncfu.ru/handle/123456789/29610
Метки:	Добавить метку Нет меток, Требуется 1-ая метка записи!

id	ir-123456789-29610
record_format	dspace
spelling	ir-123456789-296102025-02-04T09:09:10Z Synthesis of yttrium aluminum garnet ceramic powder doped with ruthenium Suprunchuk, V. E. Супрунчук, В. Е. Kravtsov, A. A. Кравцов, А. А. Tarala, L. V. Тарала, Л. В. Medyanik, E. V. Медяник, Е. В. Malyavin, F. F. Малявин, Ф. Ф. Lapin, V. A. Лапин, В. А. Bedrakov, D. P. Бедраков, Д. П. Yttrium aluminum garnet Ruthenium Alloying Ceramic powder Differential thermal analysis In the course of the work, samples of ceramic powders of yttrium-aluminum garnet doped with ruthenium ions were obtained. The introduced amount of ruthenium was 5 and 10 wt.%, respectively. The annealing temperatures were 1150 and 1600°C. In the course of the work, changes in the morphology of ceramic powders of yttrium-aluminum garnet doped with ruthenium ions were considered using scanning electron microscopy. The elemental composition was studied using energy-dispersive spectroscopy. The phase composition was investigated by X-ray phase analysis. The specific surface area of the ceramic powder was estimated using the Brunauer-Emmett-Teller method. For the obtained samples, an increase in the specific surface area of the ceramic powder with a decrease in the quantitative content of ruthenium in the system was revealed. The presence of impurity phases was established for all samples. It was found that increasing the calcination temperature to 1600°C led to a decrease in the quantitative content of impurity phases, but did not lead to their complete elimination. The sample with the closest to a single-phase composition was obtained with a ruthenium content of no more than 5 wt.% in the material. The results obtained using differential thermal analysis showed that the ruthenium content in the amounts used does not affect the kinetics of phase transitions, as well as the kinetics of mass loss of the precursor powders. 2025-02-04T09:07:24Z 2025-02-04T09:07:24Z 2024 Статья Suprunchuk, V. E., Kravtsov, A. A., Tarala, L. V., Medyanik, E. V., Malyavin, F. F., Lapin, V. A., Bedrakov, D. P. Synthesis of yttrium aluminum garnet ceramic powder doped with ruthenium // PHYSICAL AND CHEMICAL ASPECTS OF THE STUDY OF CLUSTERS NANOSTRUCTURES AND NANOMATERIALS. - 2024. - 16. - pp. 1016-1024. - DOI: 10.26456/pcascnn/2024.16.1016 https://dspace.ncfu.ru/handle/123456789/29610 ru PHYSICAL AND CHEMICAL ASPECTS OF THE STUDY OF CLUSTERS NANOSTRUCTURES AND NANOMATERIALS application/pdf Tver State University
institution	СКФУ
collection	Репозиторий
language	Russian
topic	Yttrium aluminum garnet Ruthenium Alloying Ceramic powder Differential thermal analysis
spellingShingle	Yttrium aluminum garnet Ruthenium Alloying Ceramic powder Differential thermal analysis Suprunchuk, V. E. Супрунчук, В. Е. Kravtsov, A. A. Кравцов, А. А. Tarala, L. V. Тарала, Л. В. Medyanik, E. V. Медяник, Е. В. Malyavin, F. F. Малявин, Ф. Ф. Lapin, V. A. Лапин, В. А. Bedrakov, D. P. Бедраков, Д. П. Synthesis of yttrium aluminum garnet ceramic powder doped with ruthenium
description	In the course of the work, samples of ceramic powders of yttrium-aluminum garnet doped with ruthenium ions were obtained. The introduced amount of ruthenium was 5 and 10 wt.%, respectively. The annealing temperatures were 1150 and 1600°C. In the course of the work, changes in the morphology of ceramic powders of yttrium-aluminum garnet doped with ruthenium ions were considered using scanning electron microscopy. The elemental composition was studied using energy-dispersive spectroscopy. The phase composition was investigated by X-ray phase analysis. The specific surface area of the ceramic powder was estimated using the Brunauer-Emmett-Teller method. For the obtained samples, an increase in the specific surface area of the ceramic powder with a decrease in the quantitative content of ruthenium in the system was revealed. The presence of impurity phases was established for all samples. It was found that increasing the calcination temperature to 1600°C led to a decrease in the quantitative content of impurity phases, but did not lead to their complete elimination. The sample with the closest to a single-phase composition was obtained with a ruthenium content of no more than 5 wt.% in the material. The results obtained using differential thermal analysis showed that the ruthenium content in the amounts used does not affect the kinetics of phase transitions, as well as the kinetics of mass loss of the precursor powders.
format	Статья
author	Suprunchuk, V. E. Супрунчук, В. Е. Kravtsov, A. A. Кравцов, А. А. Tarala, L. V. Тарала, Л. В. Medyanik, E. V. Медяник, Е. В. Malyavin, F. F. Малявин, Ф. Ф. Lapin, V. A. Лапин, В. А. Bedrakov, D. P. Бедраков, Д. П.
author_facet	Suprunchuk, V. E. Супрунчук, В. Е. Kravtsov, A. A. Кравцов, А. А. Tarala, L. V. Тарала, Л. В. Medyanik, E. V. Медяник, Е. В. Malyavin, F. F. Малявин, Ф. Ф. Lapin, V. A. Лапин, В. А. Bedrakov, D. P. Бедраков, Д. П.
author_sort	Suprunchuk, V. E.
title	Synthesis of yttrium aluminum garnet ceramic powder doped with ruthenium
title_short	Synthesis of yttrium aluminum garnet ceramic powder doped with ruthenium
title_full	Synthesis of yttrium aluminum garnet ceramic powder doped with ruthenium
title_fullStr	Synthesis of yttrium aluminum garnet ceramic powder doped with ruthenium
title_full_unstemmed	Synthesis of yttrium aluminum garnet ceramic powder doped with ruthenium
title_sort	synthesis of yttrium aluminum garnet ceramic powder doped with ruthenium
publisher	Tver State University
publishDate	2025
url	https://dspace.ncfu.ru/handle/123456789/29610
work_keys_str_mv	AT suprunchukve synthesisofyttriumaluminumgarnetceramicpowderdopedwithruthenium AT suprunčukve synthesisofyttriumaluminumgarnetceramicpowderdopedwithruthenium AT kravtsovaa synthesisofyttriumaluminumgarnetceramicpowderdopedwithruthenium AT kravcovaa synthesisofyttriumaluminumgarnetceramicpowderdopedwithruthenium AT taralalv synthesisofyttriumaluminumgarnetceramicpowderdopedwithruthenium AT taralalv synthesisofyttriumaluminumgarnetceramicpowderdopedwithruthenium AT medyanikev synthesisofyttriumaluminumgarnetceramicpowderdopedwithruthenium AT medânikev synthesisofyttriumaluminumgarnetceramicpowderdopedwithruthenium AT malyavinff synthesisofyttriumaluminumgarnetceramicpowderdopedwithruthenium AT malâvinff synthesisofyttriumaluminumgarnetceramicpowderdopedwithruthenium AT lapinva synthesisofyttriumaluminumgarnetceramicpowderdopedwithruthenium AT lapinva synthesisofyttriumaluminumgarnetceramicpowderdopedwithruthenium AT bedrakovdp synthesisofyttriumaluminumgarnetceramicpowderdopedwithruthenium AT bedrakovdp synthesisofyttriumaluminumgarnetceramicpowderdopedwithruthenium
_version_	1842245900978618368

Synthesis of yttrium aluminum garnet ceramic powder doped with ruthenium

Схожие документы