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Synthesis of 4,6-disubstituted 2-thioxo-1,2-dihydropyridine-3-carbonitriles by the reaction of acetylenic ketones with cyanothioacetamide

The reaction of acetylenic ketones with cyanothioacetamide in the presence of morpholine yields 4,6-disubstituted 2-thioxo-1,2-dihydropyridine-3-carbonitriles. Structure of the obtained compounds was proved using 2D NMR spectroscopy, as well as transformations into 3-aminothieno[2,3-b]pyridine-2-car...

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Hlavní autoři: Dotsenko, V. V., Доценко, В. В., Aksenova, I. V., Аксенова, И. В.
Médium: Статья
Jazyk:English
Vydáno: Pleiades Publishing 2019
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On-line přístup:https://www.scopus.com/record/display.uri?eid=2-s2.0-85068040119&origin=resultslist&sort=plf-f&src=s&st1=Synthesis+of+4%2c6-Disubstituted+2-Thioxo-1%2c2-dihydropyridine-3-carbonitriles+by+the+Reaction+of+Acetylenic+Ketones+with+Cyanothioacetamide&st2=&sid=6e4a3f0a57961460ec602538180ac367&sot=b&sdt=b&sl=152&s=TITLE-ABS-KEY%28Synthesis+of+4%2c6-Disubstituted+2-Thioxo-1%2c2-dihydropyridine-3-carbonitriles+by+the+Reaction+of+Acetylenic+Ketones+with+Cyanothioacetamide%29&relpos=0&citeCnt=0&searchTerm=
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spelling ir-20.500.12258-59742020-07-29T11:56:45Z Synthesis of 4,6-disubstituted 2-thioxo-1,2-dihydropyridine-3-carbonitriles by the reaction of acetylenic ketones with cyanothioacetamide Dotsenko, V. V. Доценко, В. В. Aksenova, I. V. Аксенова, И. В. Acetylenic ketones Bohlmann-Rahtz reaction Cyanothioacetamide Thieno-[2,3-b]pyridines Thorpe-Ziegler reaction The reaction of acetylenic ketones with cyanothioacetamide in the presence of morpholine yields 4,6-disubstituted 2-thioxo-1,2-dihydropyridine-3-carbonitriles. Structure of the obtained compounds was proved using 2D NMR spectroscopy, as well as transformations into 3-aminothieno[2,3-b]pyridine-2-carboxamide derivatives 2019-07-09T11:07:16Z 2019-07-09T11:07:16Z 2019 Статья Buryi, D.S., Dotsenko, V.V., Levashov, A.S., Lukina, D.Y., Strelkov, V.D., Aksenov, N.A., Aksenova, I.V., Netreba, E.E. Synthesis of 4,6-Disubstituted 2-Thioxo-1,2-dihydropyridine-3-carbonitriles by the Reaction of Acetylenic Ketones with Cyanothioacetamide // Russian Journal of General Chemistry. - 2019. - Volume 89. -Issue 5. - Pages 886-895 https://www.scopus.com/record/display.uri?eid=2-s2.0-85068040119&origin=resultslist&sort=plf-f&src=s&st1=Synthesis+of+4%2c6-Disubstituted+2-Thioxo-1%2c2-dihydropyridine-3-carbonitriles+by+the+Reaction+of+Acetylenic+Ketones+with+Cyanothioacetamide&st2=&sid=6e4a3f0a57961460ec602538180ac367&sot=b&sdt=b&sl=152&s=TITLE-ABS-KEY%28Synthesis+of+4%2c6-Disubstituted+2-Thioxo-1%2c2-dihydropyridine-3-carbonitriles+by+the+Reaction+of+Acetylenic+Ketones+with+Cyanothioacetamide%29&relpos=0&citeCnt=0&searchTerm= http://hdl.handle.net/20.500.12258/5974 en Russian Journal of General Chemistry application/pdf application/pdf Pleiades Publishing
institution СКФУ
collection Репозиторий
language English
topic Acetylenic ketones
Bohlmann-Rahtz reaction
Cyanothioacetamide
Thieno-[2,3-b]pyridines
Thorpe-Ziegler reaction
spellingShingle Acetylenic ketones
Bohlmann-Rahtz reaction
Cyanothioacetamide
Thieno-[2,3-b]pyridines
Thorpe-Ziegler reaction
Dotsenko, V. V.
Доценко, В. В.
Aksenova, I. V.
Аксенова, И. В.
Synthesis of 4,6-disubstituted 2-thioxo-1,2-dihydropyridine-3-carbonitriles by the reaction of acetylenic ketones with cyanothioacetamide
description The reaction of acetylenic ketones with cyanothioacetamide in the presence of morpholine yields 4,6-disubstituted 2-thioxo-1,2-dihydropyridine-3-carbonitriles. Structure of the obtained compounds was proved using 2D NMR spectroscopy, as well as transformations into 3-aminothieno[2,3-b]pyridine-2-carboxamide derivatives
format Статья
author Dotsenko, V. V.
Доценко, В. В.
Aksenova, I. V.
Аксенова, И. В.
author_facet Dotsenko, V. V.
Доценко, В. В.
Aksenova, I. V.
Аксенова, И. В.
author_sort Dotsenko, V. V.
title Synthesis of 4,6-disubstituted 2-thioxo-1,2-dihydropyridine-3-carbonitriles by the reaction of acetylenic ketones with cyanothioacetamide
title_short Synthesis of 4,6-disubstituted 2-thioxo-1,2-dihydropyridine-3-carbonitriles by the reaction of acetylenic ketones with cyanothioacetamide
title_full Synthesis of 4,6-disubstituted 2-thioxo-1,2-dihydropyridine-3-carbonitriles by the reaction of acetylenic ketones with cyanothioacetamide
title_fullStr Synthesis of 4,6-disubstituted 2-thioxo-1,2-dihydropyridine-3-carbonitriles by the reaction of acetylenic ketones with cyanothioacetamide
title_full_unstemmed Synthesis of 4,6-disubstituted 2-thioxo-1,2-dihydropyridine-3-carbonitriles by the reaction of acetylenic ketones with cyanothioacetamide
title_sort synthesis of 4,6-disubstituted 2-thioxo-1,2-dihydropyridine-3-carbonitriles by the reaction of acetylenic ketones with cyanothioacetamide
publisher Pleiades Publishing
publishDate 2019
url https://www.scopus.com/record/display.uri?eid=2-s2.0-85068040119&origin=resultslist&sort=plf-f&src=s&st1=Synthesis+of+4%2c6-Disubstituted+2-Thioxo-1%2c2-dihydropyridine-3-carbonitriles+by+the+Reaction+of+Acetylenic+Ketones+with+Cyanothioacetamide&st2=&sid=6e4a3f0a57961460ec602538180ac367&sot=b&sdt=b&sl=152&s=TITLE-ABS-KEY%28Synthesis+of+4%2c6-Disubstituted+2-Thioxo-1%2c2-dihydropyridine-3-carbonitriles+by+the+Reaction+of+Acetylenic+Ketones+with+Cyanothioacetamide%29&relpos=0&citeCnt=0&searchTerm=
https://dspace.ncfu.ru/handle/20.500.12258/5974
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