Synthesis of 4,6-disubstituted 2-thioxo-1,2-dihydropyridine-3-carbonitriles by the reaction of acetylenic ketones with cyanothioacetamide
The reaction of acetylenic ketones with cyanothioacetamide in the presence of morpholine yields 4,6-disubstituted 2-thioxo-1,2-dihydropyridine-3-carbonitriles. Structure of the obtained compounds was proved using 2D NMR spectroscopy, as well as transformations into 3-aminothieno[2,3-b]pyridine-2-car...
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Pleiades Publishing
2019
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ir-20.500.12258-59742020-07-29T11:56:45Z Synthesis of 4,6-disubstituted 2-thioxo-1,2-dihydropyridine-3-carbonitriles by the reaction of acetylenic ketones with cyanothioacetamide Dotsenko, V. V. Доценко, В. В. Aksenova, I. V. Аксенова, И. В. Acetylenic ketones Bohlmann-Rahtz reaction Cyanothioacetamide Thieno-[2,3-b]pyridines Thorpe-Ziegler reaction The reaction of acetylenic ketones with cyanothioacetamide in the presence of morpholine yields 4,6-disubstituted 2-thioxo-1,2-dihydropyridine-3-carbonitriles. Structure of the obtained compounds was proved using 2D NMR spectroscopy, as well as transformations into 3-aminothieno[2,3-b]pyridine-2-carboxamide derivatives 2019-07-09T11:07:16Z 2019-07-09T11:07:16Z 2019 Статья Buryi, D.S., Dotsenko, V.V., Levashov, A.S., Lukina, D.Y., Strelkov, V.D., Aksenov, N.A., Aksenova, I.V., Netreba, E.E. Synthesis of 4,6-Disubstituted 2-Thioxo-1,2-dihydropyridine-3-carbonitriles by the Reaction of Acetylenic Ketones with Cyanothioacetamide // Russian Journal of General Chemistry. - 2019. - Volume 89. -Issue 5. - Pages 886-895 https://www.scopus.com/record/display.uri?eid=2-s2.0-85068040119&origin=resultslist&sort=plf-f&src=s&st1=Synthesis+of+4%2c6-Disubstituted+2-Thioxo-1%2c2-dihydropyridine-3-carbonitriles+by+the+Reaction+of+Acetylenic+Ketones+with+Cyanothioacetamide&st2=&sid=6e4a3f0a57961460ec602538180ac367&sot=b&sdt=b&sl=152&s=TITLE-ABS-KEY%28Synthesis+of+4%2c6-Disubstituted+2-Thioxo-1%2c2-dihydropyridine-3-carbonitriles+by+the+Reaction+of+Acetylenic+Ketones+with+Cyanothioacetamide%29&relpos=0&citeCnt=0&searchTerm= http://hdl.handle.net/20.500.12258/5974 en Russian Journal of General Chemistry application/pdf application/pdf Pleiades Publishing |
institution |
СКФУ |
collection |
Репозиторий |
language |
English |
topic |
Acetylenic ketones Bohlmann-Rahtz reaction Cyanothioacetamide Thieno-[2,3-b]pyridines Thorpe-Ziegler reaction |
spellingShingle |
Acetylenic ketones Bohlmann-Rahtz reaction Cyanothioacetamide Thieno-[2,3-b]pyridines Thorpe-Ziegler reaction Dotsenko, V. V. Доценко, В. В. Aksenova, I. V. Аксенова, И. В. Synthesis of 4,6-disubstituted 2-thioxo-1,2-dihydropyridine-3-carbonitriles by the reaction of acetylenic ketones with cyanothioacetamide |
description |
The reaction of acetylenic ketones with cyanothioacetamide in the presence of morpholine yields 4,6-disubstituted 2-thioxo-1,2-dihydropyridine-3-carbonitriles. Structure of the obtained compounds was proved using 2D NMR spectroscopy, as well as transformations into 3-aminothieno[2,3-b]pyridine-2-carboxamide derivatives |
format |
Статья |
author |
Dotsenko, V. V. Доценко, В. В. Aksenova, I. V. Аксенова, И. В. |
author_facet |
Dotsenko, V. V. Доценко, В. В. Aksenova, I. V. Аксенова, И. В. |
author_sort |
Dotsenko, V. V. |
title |
Synthesis of 4,6-disubstituted 2-thioxo-1,2-dihydropyridine-3-carbonitriles by the reaction of acetylenic ketones with cyanothioacetamide |
title_short |
Synthesis of 4,6-disubstituted 2-thioxo-1,2-dihydropyridine-3-carbonitriles by the reaction of acetylenic ketones with cyanothioacetamide |
title_full |
Synthesis of 4,6-disubstituted 2-thioxo-1,2-dihydropyridine-3-carbonitriles by the reaction of acetylenic ketones with cyanothioacetamide |
title_fullStr |
Synthesis of 4,6-disubstituted 2-thioxo-1,2-dihydropyridine-3-carbonitriles by the reaction of acetylenic ketones with cyanothioacetamide |
title_full_unstemmed |
Synthesis of 4,6-disubstituted 2-thioxo-1,2-dihydropyridine-3-carbonitriles by the reaction of acetylenic ketones with cyanothioacetamide |
title_sort |
synthesis of 4,6-disubstituted 2-thioxo-1,2-dihydropyridine-3-carbonitriles by the reaction of acetylenic ketones with cyanothioacetamide |
publisher |
Pleiades Publishing |
publishDate |
2019 |
url |
https://www.scopus.com/record/display.uri?eid=2-s2.0-85068040119&origin=resultslist&sort=plf-f&src=s&st1=Synthesis+of+4%2c6-Disubstituted+2-Thioxo-1%2c2-dihydropyridine-3-carbonitriles+by+the+Reaction+of+Acetylenic+Ketones+with+Cyanothioacetamide&st2=&sid=6e4a3f0a57961460ec602538180ac367&sot=b&sdt=b&sl=152&s=TITLE-ABS-KEY%28Synthesis+of+4%2c6-Disubstituted+2-Thioxo-1%2c2-dihydropyridine-3-carbonitriles+by+the+Reaction+of+Acetylenic+Ketones+with+Cyanothioacetamide%29&relpos=0&citeCnt=0&searchTerm= https://dspace.ncfu.ru/handle/20.500.12258/5974 |
work_keys_str_mv |
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