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STUDY OF THE STRUCTURE AND PROPERTIES OF ZINC SILICATE STABILIZED WITH L-HISTIDINE

This paper presents the results of a study of the process of stabilization of zinc silicate nanoparticles using the amino acid L-histidine. Zinc acetate was used as a precursor, sodium silicate was used as a precipitant, and the amino acid L -histidine acted as a stabilizer. Synthesis was carried ou...

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Главные авторы: Blinova, A. A., Блинова, А. А., Maglakelidze, D. G., Маглакелидзе, Д. Г., Taravanov, M. A., Тараванов, М. А., Yasnaya, M. A., Ясная, М. А., Lapin, V. A., Лапин, В. А., Leontiev, P. S., Леонтьев, П. С.
格式: Статья
语言:Russian
出版: 2023
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在线阅读:https://dspace.ncfu.ru/handle/20.500.12258/23458
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总结:This paper presents the results of a study of the process of stabilization of zinc silicate nanoparticles using the amino acid L-histidine. Zinc acetate was used as a precursor, sodium silicate was used as a precipitant, and the amino acid L -histidine acted as a stabilizer. Synthesis was carried out by chemical precipitation in an aqueous medium. A simultaneous thermal analysis was carried out, as a result of which it was found that the addition of an amino acid to nanosized zinc silicate has a great influence on the crystal structure and thermal transitions for this material. Next, the X-ray phase analysis was carried out, which showed that of zinc silicate particles have an amorphous structure and are in a nanoscale state. At the next stage of the work, the process of interaction of an amino acid with a zinc silicate particle was studied by IR spectroscopy. The results of the study showed that stabilization of particles is accompanied by the formation of a chemical bond between silicon in the zinc silicate molecule and the amino group in the L -histidine molecule.